Preparation and Structural Characterization of 1,6-bis(N,N′-dibenzylthiocarbamoyldithio)-hexane |
Received:December 24, 2019 Revised:December 24, 2019 |
DOI:10.12136/j.issn.1000-890X.2020.09.0687 |
Key Words: crosslinking agent;anti-reversion agent;synthesis method;infrared spectrum;differential scanning calorimetry;high performance liquid chromatography;element analysis |
Author Name | Affiliation | E-mail | YANG Jiangao* | Shanxi Provincial Institute of Chemical Industry(Co.,Ltd) | yjg7231@163.com | GUO Qiaojing | Shanxi Provincial Institute of Chemical Industry(Co.,Ltd) | |
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Abstract: |
A bifunctional cross-linking agent 1,6-bis(N,N′-dibenzylthiocarbamoyldithio)-hexane was prepared by three-step method,which could be used as anti-reversion agent of diene rubber.Structure of synthetic 1,6-bis(N,N′-dibenzylthiocarbamoyldithio)-hexane was characterized by fourier transform infrared spectroscopy analysis,differential thermal scanning analysis and elemental analysis.The purity of the synthetic 1,6-bis(N,N′-dibenzylthiocarbamoyldithio)-hexane was up to 98.5% by high performance liquid chromatography analysis. |
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