Modification of carbon black by chlorination |
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DOI: |
Key Words: chlorinated carbon black;modification;structure |
Author Name | Affiliation | YANG Jin-ping | Qingdao Institute of Chemical Technology | LI Yong | Qingdao Institute of Chemical Technology | GENG Zhou | Qingdao Institute of Chemical Technology | SHEN Wei | Qingdao Institute of Chemical Technology | FU Zheng | Qingdao Institute of Chemical Technology |
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Abstract: |
The carbon black was modified by gas-solid stirring chlorination,and the chlorine content in the chlorinated carbon black as a function of the temperature and time of reaction,and the chlorine flow was investigated with the binary regressive analysis.The results showed that the suitable reaction conditions were as follows:temperature 130 ℃,time 1.5~2 h,chlorine flow 554
mL·min-1;the nitrogen-filled treatment could be used instead of the water flushing treatment for the post-treatment of chlorinated carbon black;it was indicated by SEM that the agg regated structure of the chlorinated carbon black changed,but the chain structure didnt. |
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