Continuous Determination of Zinc and Rare-earth Amounts in Rare-earth Zinc Oxide |
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DOI: |
Key Words: rare-earth zinc oxide;EDTA titrant replacement;continuous determination |
Author Name | Affiliation | Li Zhicheng | Henan Tyre Factory |
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Abstract: |
The continuous determination of zinc amd rare-earth amounts in rare-earth zinc oxide was investigarcd.The iron,aluminium and copper ions were respectively screened by ascorbic acid,sulfosalicylic acid and thiourea in an acidulous medium;the total amounrs of zinc and rare-earth were determined by titrating with EDTA titrant in hexamine buffer solution with 5.5pH till the xylenol orange indicator discolored;then EDTA in the rare-earth complex was replaced with ammonia fluoride,and the amount of rare-earth was determined with the standard zinc solurion.The method featured reliable principle,simple operation,fast determination and accurate results. |
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