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气相色谱/质谱联用鉴定胶料中防焦剂CTP的方法
Identification of Anti-scorching Agent CTP of Rubber Compounds by Gas Chromatography/Mass Spectrometry
  
DOI:
中文关键词: 气相色谱  质谱  防焦剂CTP  邻苯二甲酰亚胺
英文关键词: gas chromatography  mass spectrometry  anti-scorching agent CTP  phthalimide
基金项目:
中图分类号:TQ330.385;O675.6/7
Author NameAffiliation
GAO Jianqin Beijing Red Avenue Innovation Technology Co.Ltd 
WANG Can Beijing Red Avenue Innovation Technology Co.Ltd 
DONG Dong Beijing Red Avenue Innovation Technology Co.Ltd 
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中文摘要:
      根据防焦剂CTP与促进剂反应生成邻苯二甲酰亚胺的机理,建立气相色谱/质谱联用(GC/MS)鉴定混炼胶和硫化胶中防焦剂CTP的方法,并通过已知配方胶料验证。与红外光谱法鉴定硫化胶中防焦剂CTP相比,GC/MS法鉴定混炼胶和硫化胶中防焦剂CTP灵敏度和准确性较高,操作简单。
英文摘要:
      Based on the mechanism of the reaction of anti-scorching agent CTP and accelerator which produced phthalimide,the method of gas chromatography/mass spectrometry(GC/MS) for the identification of anti-scorching agent CTP in unvulcanized rubber and vulcanized rubber was established.It was then validated by known formulations.Compared with infrared spectroscopy(IR) method,the GC/MS method was more sensitive and accurate in the determination of anti-scorching agent CTP in unvulcanized and vulcanized rubber.
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