| 婴幼儿奶嘴中12种N-亚硝胺类物质迁移量检测的研究 |
| Determination of amount of N-nitrosamines migrated from infant nipple by GC-MS |
| 投稿时间：2016-03-03 修订日期：2016-03-03 |
| DOI： |
| 中文关键词: N-亚硝胺,气相色谱-质谱,婴幼儿奶嘴,检测 |
| 英文关键词: N-nitrosamines, GC-MS, infant nipple, determination |
| 基金项目:国家质检总局科研计划项目(2014QK208)资助。 |
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| 中文摘要: |
| 建立了婴幼儿奶嘴中12种N-亚硝基胺类物质迁移量的气相色谱-质谱联用检测方法。 样品经人工唾液盐浸提后,以二氯甲烷为溶剂萃取浸提液中的N-亚硝胺,去水浓缩后,用气相色谱-质谱联用仪进行测定,外标法定量。结果表明,方法的定量限为0.027mg/L～0.031mg/L,回收率为86.9%～120%,相对标准偏差为4.25%～8.31%,应用本方法对21 个国内外品牌的婴幼儿奶嘴进行了测试,其中16 个样品中检出了N-亚硝胺。 |
| 英文摘要: |
| A method of GC-MS for the determination of amount of 12-nitrosamines migrated from infant nipple was developed. The sample was extracted with artificial saliva solution, and the extract was purified by dichloromethane. The results showed that limit of determination (10S/N) was 0.027mg/L～0.031mg/L, recovery was 86.9%～120%,and RSD was 4.25%～8.31%(n=7). 21 domestic and foreign brands of nipple samples were tested by the above method, of which 16 samples were detected in N- nitrosamines. |
| Author Name | Affiliation | E-mail | | Chen Dewen | National Center of Quality Supervision and Inspection for Commodity,Yiwu,Zhejiang | 42030692@qq.com | | Chen Meilan | | | | Wang Zhenglin | National Center of Quality Supervision and Inspection for Commodity,Yiwu,Zhejiang | | | Gong Yuefei | National Center of Quality Supervision and Inspection for Commodity,Yiwu,Zhejiang | | | Wang Guodong | National Center of Quality Supervision and Inspection for Commodity,Yiwu,Zhejiang | | | Gong Xudong | National Center of Quality Supervision and Inspection for Commodity,Yiwu,Zhejiang | |
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