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核磁共振法测定乙烯-乙酸乙烯酯中乙酸乙烯酯含量 |
Determination of Vinyl Acetate Content in Ethylene-Vinyl Acetate by Nuclear Magnetic Resonance |
Received:November 29, 2023 Revised:November 29, 2023 |
DOI:10.12137/j.issn.2095-5448.2025.02.0106 |
中文关键词: 乙烯-乙酸乙烯酯;乙烯;乙酸乙烯酯;1H-NMR谱;13C-NMR谱;二维核磁共振谱 |
英文关键词: EVA;ethylene;vinyl acetate;1H-NMR spectrum;13C-NMR spectrum;two-dimensional NMR spectrum |
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Author Name | Affiliation | E-mail | lIU Xiaoyuan* | Stone Technology Co.,Ltd | liuxy@stonelab.com.cn | SHI Yiyi | Qingdao University of Science and Technology | | HUANG Zheng | Stone Technology Co.,Ltd | | WANG Chao | Stone Technology Co.,Ltd | | LIU Aiqin | Stone Technology Co.,Ltd | |
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中文摘要: |
采用核磁共振法测定乙烯-乙酸乙烯酯(EVA)中的乙烯和乙酸乙烯酯的相对含量。通过1H-NMR谱、13C-NMR谱和二维核磁共振谱对EVA的谱峰进行归属,选取特征峰的峰面积进行计算,分别建立1H-NMR和13C-NMR的定量方法,该方法相对于传统方法更加快速、简单。 |
英文摘要: |
The relative content of ethylene and vinyl acetate in ethylene-vinyl acetate(EVA) was determined using nuclear magnetic resonance(NMR) spectroscopy.The peaks in the EVA spectra were assigned using 1H-NMR,13C-NMR,and two-dimensional NMR spectra.Characteristic peak areas were selected for calculation and quantitative methods were established for both 1H-NMR and 13C-NMR spectra.This method was faster and simpler compared to traditional methods. |
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