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核磁共振法测定乙烯-乙酸乙烯酯中乙酸乙烯酯含量
Determination of Vinyl Acetate Content in Ethylene-Vinyl Acetate by Nuclear Magnetic Resonance
Received:November 29, 2023  Revised:November 29, 2023
DOI:10.12137/j.issn.2095-5448.2025.02.0106
中文关键词: 乙烯-乙酸乙烯酯;乙烯;乙酸乙烯酯;1H-NMR谱;13C-NMR谱;二维核磁共振谱
英文关键词: EVA;ethylene;vinyl acetate;1H-NMR spectrum;13C-NMR spectrum;two-dimensional NMR spectrum
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Author NameAffiliationE-mail
lIU Xiaoyuan* Stone Technology Co.,Ltd liuxy@stonelab.com.cn 
SHI Yiyi Qingdao University of Science and Technology  
HUANG Zheng Stone Technology Co.,Ltd  
WANG Chao Stone Technology Co.,Ltd  
LIU Aiqin Stone Technology Co.,Ltd  
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中文摘要:
      采用核磁共振法测定乙烯-乙酸乙烯酯(EVA)中的乙烯和乙酸乙烯酯的相对含量。通过1H-NMR谱、13C-NMR谱和二维核磁共振谱对EVA的谱峰进行归属,选取特征峰的峰面积进行计算,分别建立1H-NMR和13C-NMR的定量方法,该方法相对于传统方法更加快速、简单。
英文摘要:
      The relative content of ethylene and vinyl acetate in ethylene-vinyl acetate(EVA) was determined using nuclear magnetic resonance(NMR) spectroscopy.The peaks in the EVA spectra were assigned using 1H-NMR,13C-NMR,and two-dimensional NMR spectra.Characteristic peak areas were selected for calculation and quantitative methods were established for both 1H-NMR and 13C-NMR spectra.This method was faster and simpler compared to traditional methods.
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